1993 Research Publications

Crystallography Centre

Journal Articles

Adams, C.J, Bruce, M.I., Skelton, B.W. and White, A.H. A new route to complexes containing the tetracarbon (C4) ligand, Journal of Organometallic Chemistry, 450: pp C9-C11 (1993)

Adams, C.J, Bruce, M.I., Skelton, B.W. and White, A.H. Cluster chemistry LXXXVI. Metallation of pyridine in reactions with an Ru5 cluster. X-Ray structures of Ru4{m4-C2H(PPh2)} (m-PPh2)(m-NC5H4)(CO)10.CH2Cl2 and Ru6(m6-C2H)(m3-NC5H4) (m-PPh2)2(m-CO)(CO)12.1.25CHCl3, Journal of Organometallic Chemistry, 445: pp 211-217 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Cluster chemistry LXXXVIII. Reactions between Ru5(m5-C2PPh2) (m-PPh2)(CO)13 and thiols. Formation and X-ray structures of Ru5 clusters containing C2H, C2PPh2 and CCH(PPh2) ligands, Journal of Organometallic Chemistry, 452: pp 121-142 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Cluster chemistry LXXXIX. Oligomerization reactions of allene with Ru5(m5-C2PPh2)(m-PPh2)(CO)13, Journal of Organometallic Chemistry, 456: pp 113-129 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Construction of Unusual Metal Clusters using Dicarbon (C2) as a Collar. Examples based on Permetallabicyclo [2.2.0] hexane Frameworks, Journal of the Chemical Society, Chemical Communications, :5, pp 446-450 (1993)

Adams, C.J., Bruce, M.I., Horn, E., Skelton, B.W., Tiekink, E.R.T. and White, A.H. Cluster Chemistry. Part 92. Directed Syntheses and Crystal Structures of [{Ru3(CO)11}{m-PPh2[C2Co2(CO)6]C2}{Ru2- (m-PPh2) (CO)6}].CH2Cl2, [{Os3(CO)11} (m-PPh2C2C2){Co2Os3- (m-PPh2) (CO)13}] and [Co2Os3Re{m6-C2C=CH(PPh2)}(m-PPh2)- (m-CO)2(CO)14].CH2Cl2, Journal of the Chemical Society Dalton Transactions, pp 3313-3322 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Synthesis and Single-Crystal Structure Determination of Bis(carbido)bis(m-diphenylphosphido) heptadecacarbonyl-octaruthenium-Dichloromethane (1/1), Ru8(m6-C)(m5-C)(m-PPh2)2(CO)17.CH2Cl2, Australian Journal of Chemistry, 46: pp 1811-1816 (1993)

Adams, C.J., Bruce, M.I., KŸhl, O., Skelton, B.W. and White, A.H. Reactions of Ru3 clusters with functional phosphines: formation of m3-acyl and m3-imidoyl complexes, Journal of Organometallic Chemistry, 445: pp C6-C9 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Cluster chemistry LXXXIV. Reactions of Ru5(m5-C2PPh2) (m-PPh2) (CO)13 with alkenes: attack at the C2PPh2 ligand without cleavage of the C-P bond. X-ray structures of Ru5(m5-C) (m-PPh2) (m4-RC3H3PPh2) (CO)11 (R = Me, Ph) and Ru5(m5-C)(m-PPh2)(m-PhC3H3PPh2)(CO)11-n{P(OMe)3}(n = 0,1), Journal of Organometallic Chemistry, 445: pp 199-209 (1993)

Adams, C.J., Bruce, M.I., Liddell, M.J., Tiekink, E.R.T., Skelton, B.W. and White, A.H. Cluster chemistry LXXXIII. Reactions of Ru5(m5-C2PPh2) (m-PPh2)(CO)13 with olefins: Products formed by addition of an alkene to the C2 fragment. X-ray structures of Ru5(m4-PPh) {m4-C2(CHCHR)CHCH2R}(m-PPh2)(CO)12 (R = H, Me) and Ru5(m4-PPh)(m-PPh2)(m-CO) (CO)10 {h5-C5H3Me-1-(CH=CH2)-3}, Journal of Organometallic Chemistry, 445: pp 187-198 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Formal insertion of carbon into a C=C double bond on an Ru5 cluster. X-Ray structure of Ru5(m4-CC11H12)- (m3-SMe)2(m-PPh2)2(CO)9, Journal of Organometallic Chemistry, 444: pp C44-C46 (1993)

Adams, C.J., Bruce, M.I., Horn, E., Skelton, B.W., Tiekink, E.R.T. and White, A.H. Cluster Chemistry. Part 91. Clusters derived from 1,4-Bis(diphenylphosphino)buta-1, 3-diyne and Their Pyrolysis Products: A Route to Complexes containing the Tetracarbon Ligand, Journal of the Chemical Society Dalton Transactions, pp 3299-3312 (1993)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Cluster Chemistry LXXXVII. Some homo- and hetero-nuclear complexes derived from C2(PPh2)2: Crystal structures of Re3(m-H)3(m-dppa)(CO)10{dppa = C2(PPh2)2}, Re3(m-H)3(CO)11{PPh2)[m-C2Ru2(m-PPh2)(CO)6]} and Os3Ru2(m5-C2PPh2)(m-PPh2)(CO)13, Journal of Organometallic Chemistry, 447: pp 91-101 (1993)

Arbain, D., Lajis, N.H., Putra, D.P., Sargent, M.V., Skelton, B.W. and White, A.H. The Alkaloids of Ophiorrhiza cf. ferruginea, Australian Journal of Chemistry, 46: pp 969-976 (1993)

Assmus, R., Bohmer, V., Harrowfield, J.M., Ogden, M.I., Richmond, W.R., Skelton, B.W. and White, A.H. Alkali-metal Ion Complexes of the Calixarenes. Part 1. Caesium Bonding in Calix[4]arene Systems, Journal of the Chemical Society Dalton Transactions, pp 2427-2433 (1993)

Baker, L., Bowmaker, G.A., Skelton, B.W. and White, A.H. Crystal Structure, Infrared and 31p Nuclear Magnetic Resonance Studies of Complexes of Tris(2,4, 6-trimethoxyphenyl)phosphine with Mercury(II) Halides, Journal of the Chemical Society Dalton Transactions, pp 3235-3240 (1993)

Beattie, J.K., Best, S.P., Moore, F.H., Skelton, B.W. and White, A.H.Water Molecule Dispositions in the Caesium Sulfate a and b Alums: Single-Crystal Neutron Diffraction Studies of CsM(SO4)2.12H2O (M = V, Rh), Australian Journal of Chemistry, 46: pp 1337-1345 (1993)

Beckwith, A.L.J., Pyne, S.G., Dikic, B., Chai, C.L.L., Gordon, P.A., Skelton, B.W., Tozer, M.J. and White, A.H. An Efficient Synthesis of (2S)- and (2R)-N-Benzoyl-2-t-butyl-4-methyleneoxazolidin-5-one, Australian Journal of Chemistry, 46: pp 1425-1430 (1993)

Blackman, A.J., Ralph, C.E., Skelton, B.W. and White, A.H. Two Sulfur-Containing Isoquinoline Alkaloids from the Bryozoan Biflustra perfragilis, Australian Journal of Chemistry, 46: pp 213-220 (1993)

Blackman, A.J., Caiping, L., Hockless, D.C.R., Skelton, B.W. and White, A.H.Cylindricines A and B, Novel Alkaloids from the Ascidian Clavelina cylindrica, Tetrahedron, 49:38, pp 8645-8656 (1993)

Blake, A.B., Delfs, C.D., Engelhardt, L.M., Figgis, B.N., Reynolds, P.A., White, A.H., Moubaraki, B. and Murray, K.S. Magnetic Properties of Hexaammineruthenium(III) Trithiocyanate Single Crystals, Journal of the Chemical Society Dalton Transactions, pp 1417-1420 (1993)

Bowmaker, G.A., Effendy, Hanna, J.V., Healy, P.C., Skelton, B.W. and White, A.H.Crystal Structures and Spectroscopic Studies of the Mononuclear Complex [AgBr(PPh3)2] and Binuclear [Ag2X2(PPh3 )4]. 2CHCl3 (X = Cl or Br), Journal of the Chemical Society DaltonTransactions, pp 1387-1397 (1993)

Bruce, I.M., Low, P.J., Skelton, B.W. and White, A.H. Some Unusual Gold- and Rhodium-Rhenium Clusters, Journal of the Chemical Society DaltonTransactions, :20, pp 3145-3146 (1993)

Bruce, M.I., Hinterding, P., Tiekink, E.R.T., Skelton, B.W. and White, A.H.Cyclopentadienyl-ruthenium and -osmium chemistry, Journal of Organometallic Chemistry, 450: pp 209-218 (1993)

Buttner, R.H. and Maslen, E.N. Structural parameters and electron difference density in Y2BaCuO5., Acta Crystallographica, B49: pp 62-66 (1993)

Byrne, L.T., Harrowfield, J.M., Hockless, D.C.R., Peachey, B.J., Skelton, B.W. and White, A.H. Calixarene Phosphorylation: Cation Control of Reaction Pathways, Australian Journal of Chemistry, 46: pp 1673-1683 (1993)

Cavell, K.J., Jin, H., Skelton, B.W. and White, A.H. Molecular Structures of Mixed-ligand Palladium(II) and Platinum(II) Alkyl Complexes, including Three Isomorphous Compounds, Journal of the Chemical Society Dalton Transactions, pp 1973-1978 (1993)

Chappell, S.D., Engelhardt, L.M., White, A.H. and Raston, C.L.Axially asymmetric metal alkyls VIII. The ruthenium metallacycle [Ru{(2-CH2C6H4)2}(PPhMe2)3 and o-metallated [Ru{PC6H4(Me)2}X(PPhMe2)3] (X = Cl,Br), Journal of Organometallic Chemistry, 462: pp 295-300 (1993)

Cifuentes, M.P., Humphrey, M.G., Skelton, B.W. and White, A.H. Ruthenium carbonyl cluster complexes with nitrogen ligands, Journal of Organometallic Chemistry, 458: pp 211-218 (1993)

Cifuentes, M.P., Humphrey, M.G., Skelton, B.W. and White, A.H. High-Nuclearity Ruthenium Carbonyl Cluster Chemistry. Synthesis and X-ray Structure of [Ru2(m-H)(m-NC5H4)2(CO)4(NC5H5)2][Ru10(m-H)(m6-C)(CO)24], Organometallics, 12: pp 4272-4274 (1993)

Clare, B.W., Ferro, V., Skelton, B.W., Stick, R.V. and White, A.H. Approaches to the Synthesis of Retronecine from Some Pyrrolidine Precursors, Australian Journal of Chemistry, 46: pp 805-824 (1993)

Clark, I.J., Geue, R.J., Engelhardt, L.M., Harrowfield, J.MACB., Sargeson, A.M. and White, A.H. Structural Characterisation of Encapsulation Reactions Based on the Tris(ethane-1,2-diamine)cobalt(III) Ion, Australian Journal of Chemistry, 46: pp 1485-1505 (1993)

Clark, I.J., Creaser, I.I., Engelhardt, L.M., Harrowfield, J.M., Krausz, E.R., Moran, G.M., Sargeson, A.M. and White, A.H. Synthesis, Structure and Redox Properties of Nickel Complexes of Cage Amine Ligands, Australian Journal of Chemistry, 46: pp 111-126 (1993)

Creaser, I.I., Engelhardt, L.M., Harrowfield, J.M., Sargeson, A.M., Skelton, B.W. and White, A.H. Syntheses and Structures of Manganese(II) and Manganese (III) Nitrate Diaminosarcophagine Complexes, Australian Journal of Chemistry, 46: pp 465-476 (1993)

Da Cunha, E.V.L., Armstrong, J.A., Gray, A.I., Hockless, D.C.R., Waterman, P.G. and White, A.H. 3-Monoterpenyl 2,4-Dioxygenated Quinoline Alkaloids from the Aerial Parts of Eriostemon australasius subsp. banksii (Rutaceae), Australian Journal of Chemistry, 46: pp 1507-1514 (1993)

Deacon, G.B., Feng, T., Nickel, S., Skelton, B.W. and White, A.H. A Simple Synthesis of Tetrahydrofuran Complexes of Lanthanoid Trichlorides: Convenient Substitutes for Anhydrous Lanthanoid Chlorides, Journal of the Chemical Society Chemical Communications, :17, pp 1328-1329 (1993)

Deacon, G.B., Feng, T., Mackinnon, P., Newnham, R.H., Nickel, S., Skelton, B.W. and White, A.H. Organoamido- and Aryloxo-lanthanoids. V. Preparations of Low-Coordinate Lanthanoid(II) Phenolates, Ln(OC6H2But2-2,6-X-4)2(thf)n (Ln=Yb or Eu; X=H, Me or But2; n = 2 or 3) and the X-Ray Crystal Structure of Five-Coordinate [Yb(OC6H2But3-2,4,6)2(thf)3].thf, Australian Journal of Chemistry, 46: pp 387-399 (1993)

Dickson, R.S., Fallon, G.D., Greaves, B.C., Skelton, B.W. and White, A.H.Retention of dinitrogen in the reactions of some diazoalkanes with a dirhodium complex. Crystal and molecular structures of (h-C5H5)2Rh2{CF3C2CF3.CO.N2CRR'}, RR' = MePh and (t-Bu)2, Inorganica Chimica Acta, 212: pp 139-148 (1993)

Dong, Z., Pyne, S.G., Skelton, B.W. and White, A.H. Chiral Sulfur Compounds. XX. Solid State Structures and Conformations of (E) Vinyl Sulfoximines, Australian Journal of Chemistry, 46: pp 143-147 (1993)

Drok, K.J., Harrowfield, J.M., Mcniven, S.J., Sargeson, A.M., Skelton, B.W. and White, A.H. Synthesis with Chelated Imino Carboxylates: The Influence of Chelate Coligands on Reaction Pathways, Australian Journal of Chemistry, 46: pp 1557-1593 (1993)

Engelhardt, L.M., Harrowfield, J.M., Sargeson, A.M. and White, A.H. Synthesis and Structure of (1,8-Diammonio-3,6,10,13,16,19-hexaaza-bicyclo[6.6.6] icosane)nickel(II) Tetrachloride Monohydrate, Australian Journal of Chemistry, 46: pp 127-133 (1993)

Ferro, V., Skelton, B.W., Stick, R.V. and White, A.H. The Synthesis of Some Pyrrolidines as Potential Precursors to Retronecine, Australian Journal of Chemistry, 46: pp 787-803 (1993)

Ghisalberti, E.L., Hockless, D.C.R., Rowland, C.Y. and White, A.H. Structural Study of Curvularin, a Cell Division Inhibitor, Australian Journal of Chemistry, 46: pp 571-575 (1993)

Ghisalberti, E.L., Jefferies, P.R., Mori, T.A., Skelton, B.W., White, A.H. and Whiteside, N.J. Synthesis of 3,4-Dihydro-1,4-ethenonaphthalen-2(1H)-ones by Benzyne Cycloadditions, Journal of Chemical Research, pp 474-475(S) (1993)

Ghisalberti, E.L., Huo Wen, Skelton, B.W. and White, A.H. Structural Study of an ent-Kaurane Lactone, Australian Journal of Chemistry, 46: pp 743-747 (1993)

Gibbons, S., Gray, A.I., Hockless, D.C.R., Lavaud, C., Nuzillard, J., Massiot, G., Waterman, P.G. and White, A.H. D:A-Friedo-Oleanane Triterpenes from the Stem Bark of Phyllobotryon spathulatum, Phytochemistry, 34:1, pp 273-277 (1993)

Hakim, E.H., Achmad, S.A., Effendy, Ghisalberti, E.L., Hockless, D.C.R. and White, A.H. Structural Studies of Three Sesquiterpenes from Litsea spp. (Lauraceae), Australian Journal of Chemistry, 46: pp 1355-1362 (1993)

Hall, S.R. and Sievers, R. CIF Applications I. QUASAR: for Extracting Data from a CIF, Journal of Applied Crystallography, 26: pp 469-473 (1993)

Hall, S.R. CIF Applications II. CIFIO: for CIF Input/Output in the Xtal System, Journal of Applied Crystallography, 26: pp 474-479 (1993)

Hall, S.R. CIF Applications III. CYCLOPS: for Validating CIF Data Names, Journal of Applied Crystallography, 26: pp 480-481 (1993)

Hall, S.R. CIF Applications IV. CIFtbx: A Tool Box for Manipulating CIFs, Journal of Applied Crystallography, 26: pp 482-494 (1993)

Harrowfield, J.M., Skelton, B.W. and White, A.H. Lewis-base Adducts of Lead(II) Complexes. Part 6. X-Ray Structural Characterisation of Adducts of Lead(II) Bis(perchlorate) with Dimethyl Sulfoxide, Journal of the Chemical Society Dalton Transactions, pp 2011-2016 (1993)

Harrowfield, J.M., Ogden, M.I., Richmond, W.R., Skelton, B.W. and White, A.H Cation-Calixarene Interactions: Tetraalkylammonium Cation Binding by Calixarene Anions, Journal of the Chemical Society Perkin Transactions 2, pp 2183-2190 (1993)

Hester, J.R., Maslen, E.N., Glazer, A.M. and Stadnicka, K. Jahn-Teller distortion of the electron density in a-nickel sulfate hexahydrate, Acta Crystallographica, B49: pp 641-646 (1993)

Hester, J.R., Maslen, E.N., Spadaccini, N., Ishizawa, N. and Satow, Y.Electron density in potassium tetrachloropalladate (K2PdCI4) from synchrotron radiation data, Acta Crystallographica, B49: pp 842-846 (1993)

Hester, J.R., Maslen, E.N., Spadaccini, N., Ishizawa, N. and Satow, Y.Accurate synchrotron radiation Dp maps for K2Si6 and K2PdCIl, Acta Crystallographica, B49: pp 967-973 (1993)

Jolly, B.S., Lappert, M.F., Engelhardt, L.M., White, A.H. and Raston, C.L.Subvalent Group 14 Metal Compounds. Part 16. Synthesis, Crystal Structure and Characterisation of Some b-Functionalised-alkyltin(II) Complexes, SnR(X) {R = C5H4N[C(SiMe3)2] -2; X = R, Cl or N(SiMe3)2}, Journal of the Chemical Society Dalton Transactions, pp 2653-2663 (1993)

Lee, J., Humphrey, M.G., Hockless, D.C.R., Skelton, B.W. and White, A.H.Mixed-Metal Cluster Chemistry. Site-Selective Reactions of CpWIr3(CO)11 with PPh3 and Bidentate Phosphines: X-ray Crystal Structures of CpWIr3(m-dppe)(m-CO)3(CO)6, CpWIr3(m-dppm)(m-CO)3(CO)6, and CpWIr3(m-dppa)(m-CO)3(CO)6, Organometallics, 12: pp 3468-3473 (1993)

Lindoy, L.F., Skelton, B.W., Smith, S.V. and White, A.H. New Macrocyclic Ligands. III Pendant 2-Pyridylmethyl and Diethylaminoethyl Arm Derivatives of Dibenzo-Substituted O2N2-Donor Rings. The X-ray Structure of a Pendant 2-Pyridylmethyl Derivative, Australian Journal of Chemistry, 46: pp 363-375 (1993)

Maslen, E.N., Spadaccini, N., Ito, T., Marumo, F., Tanaka, K. and Satow, Y. A synchrotron radiation study of potassium zinc fluoride perovskite, Acta Crystallographica, B49: pp 632-636 (1993)

Maslen, E.N. and Spadaccini, N. Extinction corrections from equivalent reflections, Acta Crystallographica, A49: pp 661-667 (1993)

Maslen, E.N., Streltsov, V.A. and Streltsova, N.R. X-ray study of the electron density in magnesite, MgCO3, Acta Crystallographica, B49: pp 980-984 (1993)

Maslen, E.N., Streltsov, V.A., Streltsova, N.R., Ishizawa, N. and Satow, Y.Synchrotron X-ray study of the electron density in a-Al2O3, Acta Crystallographica, B49: pp 973-980 (1993)

Maslen, E.N., Streltsov, V.A. and Streltsova, N.R. X-ray study of the electron density in calcite, CaCO3, Acta Crystallographica, B49: pp 636-641 (1993)

Prawat, U., Tuntiwachwuttikul, P., Taylor, W.C., Engelhardt, L.M., Skelton, B.W. and White, A.H. Diterpenes from a Kaempferia species, Phytochemistry, 32: pp 991-997 (1993)

Pyne, S.G., Dikic, B., Gordon, P.A., Skelton, B.W. and White, A.H. Asymmetric Synthesis of Chiral Cyclic Amino Acids by Diels-Alder Reactions of (2S)- and (2R)-4-Methyleneoxazolidin-5-ones, Australian Journal of Chemistry, 46: pp 73-93 (1993)

Shaari, K., Gray, A.I., Hockless, D.C.R., Waterman, P.G. and White, A.H.Structural Study of Kaurane Diterpenes from Ryparosa acuminata (Flacourtiaceae), Australian Journal of Chemistry, 46: pp 739-742 (1993)

Streltsov, V.A., Belokoneva, E.L., Tsirelson, V.G. and Hansen, N. Multipole Analysis of the Electron Density in Triphylite LiFePO4 using X-ray Diffraction Data, Acta Crystallographica, B49: pp 147-153 (1993)

Thinapong, P., Pohmakotr, M., Skelton, B.W. and White, A.H. Structures of Two Diastereomers of 1-(a-Hydroxy-m-methoxybenzyl)-1-(phenylsulfinyl)cyclopropane, Acta Crystallographica, C49: pp 54-57 (1993)

Others

Du Boulay, D. and Maslen, E.N. Absorption, extinction and dead-time correction for high precision imaging with synchrotron sources, XVI Congress of the International Union of Crystallography, A49: p 376, Beijing (1993)

Etschmann, B.E., Maslen, E.N. and Streltsova, N.R. Deformation densities in simple rare earth compounds, XVI Congress of the International Union of Crystallography, A49: p 382, Beijing (1993)

Hall, S.R. Advances in Global Databases and Common Data Exchange Formats, XVI Congress of the International Union of Crystallography, A49: pp 414-414, Beijing (1993)

Hall, S.R. The CIF DDL Dictionary and its role in CIF Software Applications, XVI Congress of the International Union of Crystallography, A49: p 413, Beijing (1993)

Hester, J., Hsu, R. and Maslen, E.N. Second-nearest-neighbour interactions and the electron density in Y2BaCuO5, XVI Congress of the International Union of Crystallography, A49: pp 381-382, Beijing (1993)

Maslen, E.N. When automatic structure solution fails, XVI Congress of the International Union of Crystallography, A49: pp 138-139, Beijing (1993)

Maslen, E.N., Streltsov, V.A. and Streltsova, N.R. X-ray study of the electron density in rhombohedral carbonates CaCO3, MgCO3, MnCO3, XVI Congress of the International Union of Crystallography, A49: pp 382-383, Beijing (1993)

Stewart, J.M., Hall, S.R., Watenpaugh, K.D., Flack, H.D., Collins, D.M. and Grossie, D.A. Xtal 3.2: A Crystallographic Software System, XVI Congress of the International Union of Crystallography, A49: pp 56-57, Beijing (1993)

Toby, B.H., Langford, J.I. and Hall, S.R. A Universal File Format for Powder Diffraction Data Archive and Interchange: The IUCR Crystallographic Information File Format, XVI Congress of the International Union of Crystallography, A49: p 410, Beijing (1993)