1997 Research Publications

Crystallography Centre

Journal Articles

Abidi, R., Harrowfield, J.M., Skelton, B.W., White, A.H., Asfari, Z. and Vicens, J. Synthesis, Structure and Alkali Metal Ion Binding Properties of a Podand Polyether Derived from Calix[4]arene, 5,11,17,23-tetra-tert-butyl-25,27-di(phenylmethoxy)-26,28-di(2'-methoxyethoxy)-calix[4]arene, Journal of Inclusion Phenomena and Molecular Recognition in Chemistry, 27: pp 291-302 (1997)

Adam, K.R., Atkinson, I.M., Davis, R.L., Lindoy, L.F., Mahinay, M.S., McCool, B.J., Skelton, B.W. and White, A.H. Self-assembly directed by NH...O hydrogen bonding: a neutron study of a trilayered supramolecular array formed between 1,2-diaminoethane and benzoic acid, Chemical Communications, pp 467-468 (1997)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Reactions of [Ru5(m5-C2PPh2)(m-PPh2)(CO)13] with dimethyl disulfide. Synthesis of an open Ru5 cluster containing the dicarbon (C2) ligand and related chemistry, Journal of Chemical Society, DaltonTransactions, pp 2937-2948 (1997)

Adams, C.J., Bruce, M.I., Skelton, B.W., White, A.H., Frapper, G. and Halet, J-F. Reaction of a dicarbon Ru5 cluster with CO: crystal structures of [Ru5 (m4-C2)(m-SMe)2(m-PPh2)2(CO)13] and [Ru4(m4-C2)(m-SMe)2-(m-PPh2)2(CO)10]*, Journal of the Chemical Society, DaltonTransactions, pp 371-375 (1997)

Adams, M.C., Koutsantonis, G.A., Skelton, B.W. and White, A.H. Iron-substituted arsine, [Fe(AsPh2(dppe)(h-C5H5)].2thf (dppe = pH2PCH2CH2PPh2, thf = tetrahydrofuran), Journal of the Chemical Society, DaltonTransactions, pp 3483-3485 (1997)

Affandi, D., Berners-Price, S.J., Effendy, Harvey, P.J., Healy, P.C., Ruch, B.E. and White, A.H. Influence of anion on the solution and solid-state structures of some 1:2 adducts of silver(I) salts with 1,3-bis(diphenylphosphino)propane, Journal of the Chemical Society, Dalton Transactions, pp 1411-1420 (1997)

Andrews, P.C., Raston, C.L., Skelton, B.W. and White, A.H. Self-assembling polymeric mixed donor (O/N) N-ethylmorpholine adducts of alane (AEH3), Chemical Communications, pp 245-246 (1997)

Andrews, P.C., Raston, C.L., Skelton, B.W. and White, A.H. A gem-aluminium(III)/antimony(III) C centre incorporated in a bimetallic six-membered heterocycle, Chemical Communications, pp 1183-1184 (1997)

Armanasco, N.L., Baker, M.V., North, M.R., Skelton, B.W. and White, A.H. Chromium(0) tricarbonyl complexes of 1,3,5-triazacyclohexanes, Journal of the Chemical Society, DaltonTransactions, pp 1363-1368 (1997)

Astley, T., Hitchman, M.A., Skelton, B.W. and White, A.H. Structure, electronic spectrum and angular-overlap bonding parameters of Bis[bis(pyrazol-1-yl)(2-thienyl)-methane](nitrato-O,O')nickel(II) Nitrate, Australian Journal of Chemistry, 50: pp 145-148 (1997)

Baker, R.W., Liu, S., Sargent, M.V., Skelton, B.W. and White, A.H. Absolute stereochemistry of 1,2'-linked bi(naphthoquinone)s, Chemical Communications, pp 451-452 (1997)

Baker, R.W., Liu, S., Sargent, M.V., Skelton, B.W. and White, A.H. Regioselectivity in the Lithiation of 1,3-Disubstituted Arenes, Australian Journal of Chemistry, 50: pp 831-840 (1997)

Bilyk, A., Harrowfield, J.M., Skelton, B.W. and White, A.H. Rhodium-catalysed hydrogenation of calix[4]arene, Anales de Quimica International Edition, 93: pp 363-370 (1997)

Bilyk, A., Harrowfield, J.M., Skelton, B.W. and White, A.H. Partically reduced calix[4]arenes: structures and co-ordination chemistry, Journal of the Chemical Society, DaltonTransactions, pp 4251-4256 (1997)

Bowmaker, G.A., Effendy, Hart, R.D., Kildea, J.D., de Silva, E.N. and White, A.H.Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXXI Synthesis, Spectroscopy and Structural Systematics of Some 1:2 Binuclear Adducts of Silver(I) Compounds with Triphenylarsine, [(Ph3As)2Ag(m-X)2Ag(AsPh3)2], X = Cl, Br, I, SCN, Australian Journal of Chemistry, 50: pp 627-640 (1997)

Bowmaker, G.A., Effendy, Kildea, J.D. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXVII Synthesis, Spectroscopy and Structural Systematics of Some 1:3 Adducts of Silver(I) Compounds with Triphenylarsine, [(Ph3As)3AgX], X = Cl, Br, I, SCN, Australian Journal of Chemistry, 50: pp 577-586 (1997)

Bowmaker, G.A., Hart, R.D., de Silva, E.N., Skelton, B.W. and White, A.H.Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXV Synthesis, Spectroscopy and Structural Systematics of Some 1:3 Adducts of Copper(I) Compounds with Triphenylarsine, [(Ph3As)3CuX], X = Cl, Br, I, ONO2, Australian Journal of Chemistry, 50: pp 553-565 (1997)

Bowmaker, G.A., Hart, R.D., de Silva, E.N., Skelton, B.W. and White, A.H.Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXX Synthesis, Spectroscopy and Structural Systematics of 1:2 Binuclear Adducts of Copper(I) Halides with Triphenylstibine, [(Ph3Sb)2Cu(SbPh3]2, X = Cl, Br, I, Australian Journal of Chemistry, 50: pp 621-626 (1997)

Bowmaker, G.A., Hart, R.D. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXVI Synthesis, Spectroscopy and Structural Systematics of Some 1:3 Adducts of Copper(I) Compounds with Triphenylstibine, [(Ph3Sb)3CuX], X = Br, I, ONO2, Australian Journal of Chemistry, 50: pp 567-576 (1997)

Bowmaker, G.A., Effendy, de Silva, E.N. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXXII Synthesis, Spectroscopy and Structural Systematics of Some 1:2 Binuclear Complexes of Silver(I) Halides with Triphenylstibine, [(Ph3Sb)2Ag(m-X)2Ag(SbPh3)2], X = Cl, Br, I,, Australian Journal of Chemistry, 50: pp 641-651 (1997)

Bowmaker, G.A., Hart, R.D., Kildea, J.D., de Silva, E.N., Skelton, B.W. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXIX Syntheses, Spectroscopy and Structural Systematics of Some (Solvated) 1:2 Binuclear Adducts of Copper(I) Compounds with Triphenylarsine, [(Ph3As)2Cu(m-X)2Cu(AsPh3)2], X = Cl, Br, ONO2, Australian Journal of Chemistry, 50: pp 605-619 (1997)

Bowmaker, G.A., Effendy, Hart, R.D., Kildea, J.D., de Silva, E.N., Skelton, B.W. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXIV Syntheses, Spectroscopy and Structures of Some 1:4 Adducts of Copper(I) and Silver(I) Perchlorates with Triphenylarsine and Triphenylstibine, Australian Journal of Chemistry, 50: pp 539-552 (1997)

Bowmaker, G.A., Effendy, Hart, R.D., Kildea, J.D. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXXIII Synthesis, Spectroscopy and Structural Systematics of New 1:1 'Cubane' Tetramers of Copper(I) and Silver(I) Halides with Triphenylarsine, Australian Journal of Chemistry, 50: pp 653-670 (1997)

Britovsek, G.J.P., Cavell, K.J., Green, M.J., Gerhards, F., Skelton, B.W. and White, A.H. Cationic methyl-palladium(II) complexes containing bidentate N^O and P^O ligands and a tridentate P^O^N ligand: synthesis, carbonylation and catalytic applications in the copolymerisation of carbon monoxide and ethene, Journal of Organometallic Chemistry, 533: pp 201-212 (1997)

Bruce, M.I., Hinterding, P., Mingzhe, K., Low, P.J., Skelton, B.W. and White, A.H. Cycloaddition of aromatic imines to a ruthenium butatrienylidene complex: synthesis of4-ethynylquinoline and 1-azabuta-1,3-diene complexes, Chemical Communications, pp 715-716 (1997)

Bruce, M.I., Zaitseva, N.N., Skelton, B.W. and White, A.H. Preparation and thermolysis of complexes derived from some trinuclear ruthenium clusters and 1,4-diphenylbuta-1,3-diyne, Journal of Organometallic Chemistry, 536-537: pp 93-107 (1997)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Crystal and molecular structures of Ru3(CO)12-n(PMe3)n) (n=1, 2), Australian Journal of Chemistry, 50: pp 163-168 (1997)

Bruce, M.I., Surynt, R.J., Skelton, B.W. and White, A.H. Formation of a Metallabicyclo[10.3.0]pentadecatriene system: molecular structure of Ru3(m3-C2Ph2C12H16)(m-CO)2(CO)6, Australian Journal of Chemistry, 50: pp 701-704 (1997)

Bruce, M.I., Humphrey, P.A., Skelton, B.W. and White, A.H. Coupling of acetylide and C2 fragments during cluster condensation: pyrolysis of [{Ru3(m-H)(m3-C2Bu')(CO)8}2(-dppa)][dppa = C2PPh2)2], Journal of the Chemical Society, Dalton Transactions, pp 1485-1487 (1997)

Bruce, M.I., Humphrey, P.A., Skelton, B.W. and White, A.H. Trapping of a phenyl group by a ruthenium cluster duing dephenylation of coordinated CH2(PPh2)2(dppm), Journal of Organometallic Chemistry, 539: pp 141-146 (1997)

Bruce, M.I., Humphrey, P.A., Skelton, B.W. and White, A.H. Acetylenic phosphines bridging two cluster units: molecular structure of {Ru3(m-H)(m3-C2But)(CO)8}2(m-dppa)[dppa = C2(PPh2)2], Australian Journal of Chemistry, 50: pp 535-538 (1997)

Bruce, M.I., Humphrey, P.A., Skelton, B.W. and White, A.H. Some Au3Ru3 clusters. X-ray structures of Ru3(m3-CMeCHCMe)(CO)8{Au3(PPh3)3} and Ru3(m3-C2Ph)(CO)8{Au3(PPh3)3}, Journal of Organometallic Chemistry, 545-546: pp 207-218 (1997)

Byrne, L.T., Johnson, J.A., Koutsantonis, G.A., Skelton, B.W. and White, A.H. Novel synthesis of two tert-butyl ketenyl phosphinidine ligands on a trinuclear ruthenium framework. X-Ray structure determination of [Ru(m-dppm)(CO)7{m3-PC(=C=O)But}2], Chemical Communications, pp 391-392 (1997)

Canty, A.J., Traill, P.R., Skelton, B.W. and White, A.H. Alkene analogues of bis(N-donor)ketone ligands: ruthenium(II) complexes containing 1-(pyridin-2-yl)-1-(N-methylimidazol-2-yl)ethene and 1,1-bis(N-methylimidazol-2-yl)ethene ((mim)2C=CH2), and structural studies of [Ru(bpy)2{(mim)2C=CH2}][PF6]2 complex [Ru(bpy)2(pyCO2)][PF6], Inorganica Chemica Acta, 255: pp 117-123 (1997)

Canty, A.J., Fritsche, S.D., Hong, J., Patel, J., Skelton, B.W. and White, A.H.Water and Protic Acids as Oxidants for Platinum(II): Diorgano(hydrido)platinum(IV) and Diorgano(hydroxo)platinum(IV) Chemistry, Including Structural Studies of Poly(pyrazol-1-yl)borate Complexes Pt(OH)R2{(pz)3BH}(R=Methyl,p-Tolyl) and Pt(OH)Me2{(pz)4B}.H2O, Organometallics, 16: pp 2175-2182 (1997)

Coutinho, K.J., Dickson, R.S., Fallon, G.D., Jackson, W.R., de Simone, T., Skelton, B.W. and White, A.H. Isolation and characterization of hydroformylation 'intermediates' from stoichiometric reactions between phosphinoalkenes and some heterobinuclear complexes, Journal of the Chemical Society, Dalton Transactions, pp 3193-3199 (1997)

Deacon, G.B., Feng, T., Junk, P.C., Skelton, B.W. and White, A.H. Novel Low-Coordinate Lanthanoid(II) and -(III) Aryloxide Complexes - the X-Ray Structures of Bis(2,6-diphenylphenolato)tris(tetrahydrofuran)-ytterbium(II), Bis(1,2-dimethoxyethane)bis(2,6-diphenylphenolato)ytterbium(II), and 1,2-Dimethoxyethanetris(2,6-diphenylphenolato)ytterbium(III) and -neodymium(III), Chemische Berichte, 130: pp 851-857 (1997)

Deacon, G.B., Forsyth, C.M., Gatehouse, B.M., Philosof, A., Skelton, B.W., White, A.H. and White, P.A. Organolanthanoids. XXI, Australian Journal Chemistry, 50: pp 959-970 (1997)

Deacon, G.B., Feng, T., Hockless, D.C.R., Junk, P.C., Skelton, B.W. and White, A.H. A tetranuclear neodymium cage which tightly binds sodium carbonate molecules, Chemical Communications, pp 341-342 (1997)

Deacon, G.B., Feng, T., Junk, P.C., Skelton, B.W. and White, A.H. Homoleptic anionic aryloxolanthanoid(III) complexes, Journal of the Chemical Society, DaltonTransactions, pp 1181-1186 (1997)

Desjardins, S.Y., Cavell, K.J., Hoare, J.L., Skelton, B.W., Sobolev, A.N., White, A.H. and Keim, W. Single component N-O chelated arylnickel(II) complexes as ethene polymerisation and CO/ethene copolymerisation catalysts. Examples of ligand induced changes to the reaction pathway., Journal of Organometallic Chemistry, 544: pp 163-174 (1997)

Dong, Z., Pyne, S.G., Skelton, B.W. and White, A.H. One-pot Annulation of Enones with Lithiated Allyl Phenyl Sulfone, E.C., pp 103-104 (1997)

Effendy, Grigsby, W.J., Hart, R.D., Raston, C.L., Skelton, B.W. and White, A.H.Structural Characterization of Some Novel Oxidation Products of Triphenylstibine, Australian Journal of Chemistry, 50: pp 675-681 (1997)

Effendy, Kildea, J.D. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds. LXXIV Synthesis and Structure of the 1:1 Adduct of Silver(1) Nitrate with Triphenylstibine, Australian Journal of Chemistry, 50: pp 671-674 (1997)

Effendy, Kildea, J.D. and White, A.H. Lewis-Base Adducts of Group 11 Metal(I) Compounds; LXVIII Synthesis and Structural Systematics of Some 1:3 Adducts of Silver(I) Compounds with Triphenylstibine, [(Ph3Sb)3AgX], X = Cl, I, SCN, NCS, CN, ONO2, Australian Journal of Chemistry, 50: pp 587-604 (1997)

Fairlie, D.P., Jackson, W.G., Skelton, B.W., Wen, H., White, A.H., Wickramasinghe, W.A., Woon, T.C. and Taube, H.Models for Arginine-Metal Binding. Synthesis of Guanidine and Urea Ligands through Amination and Hydration of a Cyanamide Ligand Bound to Platinum(II), Osmium(III), and Cobalt(III), Inorganic Chemistry, 36:6, pp 1020-1028 (1997)

Gardiner, M.G., Raston, C.L., Skelton, B.W. and White, A.H. Atomic and Neutral Aluminum Bis(N,N'-di-tert-butylethylenediamide) Complexes:[A1{[N(t-Bu)CH2]2}2]- and [A1{[N(t-Bu)CH2]2}2], Inorganic Chemistry, 36: pp 2795-2803 (1997)

George, A.V., Hockless, D.C.R., Skelton, B.W., Field, L.D., Malouf, E.Y., McQueen, A.E.D., Pike, S.R., Purches, G.R., Hambley, T.W., Buys, I.E. and White, A.H.Synthesis and characterisation of nitrile complexes of iron, Journal of Organometallic Chemistry, 538: pp 101-110 (1997)

Glaum, M., Klaui, W., Skelton, B.W. and White, A.H. Synthesis, X-ray crystal structure and reactivity of [(tmeda)(p-tolyl)Pd(m2-I)AgL], an unusual silver iodide complex; reversible CO insertion into the Pd-C Bond of [Pd(PPh3)(p-tolyl)L](L- = [(C5H5)Co{P(OR)20}3]-, R = Me, Pri), Australian Journal of Chemistry, 50: pp 1047-1052 (1997)

Godfrey, P.D., Raston, C.L., Skelton, B.W., Tolhurst, V-A and White, A.H.Approaching a cluster of aluminium(III) selenide: [A14Se5(H)2(NMe3)4], Chemical Communications, pp 2235-2236 (1997)

Hsu, R., Maslen, E.N., Du Boulay, D. and Ishizawa, N. Synchrotron X-ray Studies of LiNbO3 and LiTaO3, Acta Crystallographica Section B, 53:ISSN 0108-7681, pp 420-428 (1997)

Khan, K., Raston, C.L., McGrady, J.E., Skelton, B.W. and White, A.H.Hydride-Bridged Heterobimetallic complexes of Zirconium and Aluminum, Organometallics, 16: pp 3252-3254 (1997)

Lappert, M.F., Raston, C.L., Skelton, B.W. and White, A.H. C-Centred chiral metal alkyls, [MR(Cl)(h-C5H5)2], rac- and meso-[ZrR2(h-C5H5)2] [R = CH(SiMe3)C6H4Me-o], and their one-electron reductions; reaction of Li[CH(SiMe3)2]-(Me2NCH2CH2NMe2) with [MC12(h-C5H5)2](M = Zr or Hf), Journal of the Chemical Society, Dalton Transactions, pp 2895-2902 (1997)

McAuliffe, J.C., Skelton, B.W., Stick, R.V. and White, A.H. b-Acarbose. IV., Australian Journal of Chemistry, 50: pp 209-218 (1997)

Petrusenko, S.R., Kokozay, V.N., Vassilyeva, O.YU. and Skelton, B.W.Three-dimensional structure of the clathrate complex [{Ni(NCS)2(H2O2)(dabco)2}.dabco].2dmso obtained from zero valent metal (dabco = 1,4-diazabicyclo[2.2.2]octane and dmso = dimethyl sulfoxide), Journal of the Chemical Society, DaltonTransactions, pp 1793-1794 (1997)

Pyne, S.G., Dong, Z., Skelton, B.W. and White, A.H. Cyclopropanation reactions of Enones with Lithiated Sulfoximines: Application to the asymmetric synthesis of Chiral Cyclopropanes, Organometallic Chemistry, 62: pp 2337-2343 (1997)

Pyne, S.G., Dong, Z., Skelton, B.W. and White, A.H. Reactions of Lithiated N-Tosyl S-Phenyl S-2-Propenyl Sulfoximine with Aldehydes, Sulfur Letters, 20: pp 255-260 (1997)

Pyne, S.G., Hellmund, K.A., Skelton, B.W. and White, A.H. The reaction of a-phenylsulfinyl- and a-phenylsulfonylacrylates with nitrogen nucleophiles, Sulfur Letters, 20:6, pp 249-254 (1997)

Pyne, S.G., Schafer, K., Skelton, B.W. and White, A.H. Synthesis of novel conformationally restricted L-glutamate analogues, Chemical Communications, pp 2267-2268 (1997)

Raabe, G., Hall, S.R., Thomas, H.G., Wellen, U. and Simons, J. (1RS,3SR,4RS,5RS,7SR,9SR)-4,7-Diacetyl-9-hydroxy-1,3,5,9-tetramethyl-2,6,8-trioxatri-cyclo[3.2.1.13,7]nonane: a tricyclic system formed under cathodic conditions, Acta Crystallographica Section C, 53:ISSN 0108-2701, pp 1107-1111 (1997)

Syah, Y.M., Ghisalberti, E.L., Skelton, B.W. and White, A.H. A New Class of Tricyclic Deterpenes from Eremophila georgei (Myoporaceae), Australian Journal of Chemistry, 50: pp 705-709 (1997)

Syah, Y.M., Ghisalberti, E.L., Skelton, B.W. and White, A.H. Three New Sesquiterpene Butenolides from Eremophila Species, Journal of Natural Products, 60: pp 49-51 (1997)

Conference Publications

Hall, S.R. The Role of Data Tagging and Dictionaries in Modelling Databases, Third Australian Molecular Modelling Workshop, Melbourne, Australia, CRC, p 14 L7 (1997)

Hall, S.R. Electronic Publishing and Future Data Access, CRYSTAL XX, The Twentieth Meeting of the Society of Crystallographers in Australia, Australia, Society of Crystallographers in Australia, pp D2-AM, O-07 (1997)

Hall, S.R. XTAL_GX AND XTAL3.5: New Software Releases, Crystal XX. The Twentieth Meeting of the Society of Crystallographers in Australia, Australia, Society of Crystallographers in Australia, pp P-10 046 (1997)

Maslen, E.N. and Streltsov, V.A. Electron Difference Densities in DyFe2 and HoFe2, Crystal XX. The Twentienth Meeting of the Society of Crystallographers in Australia, Queenstown, New Zealand, Society of Crystallographers in Australia, pp P-04 (1997)

O'Toole, N.J., Maslen, E.N. and Streltsov, V.A. Structural effects of the electron density in CoF2 and ZnF2, Crystal XX. The Twentieth Meeting of the Society of Crystallographers in Australia, Queenstown, New Zealand, Society of Crystallographers in Australia, pp P-05/031 (1997)

O'Toole, N.J., Maslen, E.N. and Streltsov, V.A. The Calculation of Mean Inner Potentials from X-ray Diffraction Data, Sagamore XII Conference, Commision on Charge, Spin and Momentum Densities, University of Regina, International Union of Crystallography, p PA73 (1997)

Streltsov, V.A. Electron density imaging with synchrotron X-radiation, Crystal XX. The Twentieth Meeting of the Society of Crystallographers in Australia, Queenstown, New Zealand, Society of Crystallographers in Australia, pp D2-AM/O-04 (1997)

Streltsov, V.A. Synchrotron Electron Densities in RFe2 (R=Rare Earth), Sagamore XII Conference, Commision on Charge, Spin and Momentum Densities, University of Regina, International Union of Crystallography, p WP46 (1997)

Streltsov, V.A. and Maslen, E.N. Synchrotron electron density probe of intermediate valence and heavy fermion systems, Crystal XX. The Twentieth Meeting of Society of Crystallographers in Australia, Queenstown, New Zealand, Society of Crystallographers in Australia, pp P-03/029 (1997)

Others

Streltsov, V.A., Maslen, E.N. and Ishizawa, N. Synchrotron electron density for intermetallic rare earth compounds, Photon Factory Activity Report 1996, 14:14, p 312, Japan (1997)