1999 Research Publications

Crystallography Centre

Journal Articles

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Reactions of Ru5(m5-C2)(m-SMe)2(m-PPh2)2(CO)11 with disubstituted alkynes C2R2 (R = Me, Ph), Journal of the Chemical Society, DaltonTransactions, pp 1283-1288 (1999)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Reactions of the cluster complex [Ru5(µ5-C2)(µ-SMe)2(µ-PPh2)2(CO)11] with terminal alkynes HCšCR (R = Ph, But, SiMe3), Journal of the Chemical Society Dalton Transactions, pp 2451-2459 (1999)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Synthesis and structure of Ru5(µ5-C2PPh2)(µ-dppm)(µ-PPh2)(CO)11.thf, Australian Journal of Chemistry, 52: pp 409-411 (1999)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Cyclo-addition of buta-1,3-dene to cluster-bound dicarbon: X-ray structure of Ru5(µ3-C6H6)(µ3-SMe)2(µ-PPh2)2(CO)10, Journal of Organometallic Chemistry, 573: pp 134-138 (1999)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Double addition of a 1,3-diyne to C2 on an Ru5 cluster gives a multi-branched C10 chain, Journal of Organometallic Chemistry, 589: pp 213-221 (1999)

Adams, C.J., Bruce, M.I., Skelton, B.W. and White, A.H. Reactions of Ru5(µ5-C2)(µ-SMe)2(µ-PPh2)2(CO)11 with C2(SiMe3)2: formation of butatrienylidene complexes and related chemistry. X-ray crystal structures of Ru5{µ5-CC[C2(SiMe3)]C(SiMe3)C(SiMe3)}(µ3-SMe)(µ-PPh2)2(CO)10, Ru5(µ5-CCCCH2)(µ3-SMe)(µ-SMe)(µ-PPh2)2(CO)10 and Ru5(µ5-CCCCH2)(µ-SMe)2(µ-PPh2)2(CO)11, Journal of Organometallic Chemistry, 584: pp 254-264 (1999)

Almgren, J., Streltsov, V.A., Sobolev, A.N., Figgis, B.N. and Albertsson, J.Structure of and electron density in RbTiOAsO4 at 9.6 K, Acta Crystallographica Section B, B55: pp 712-720 (1999)

Andrews, P.C., Atwood, J.L., Barbour, L.J., Croucher, P.D., Nichols, P.J., Smith, N.O., Skelton, B.W., White, A.H. and Raston, C.L. Supramolecular confinement of C60,S8,P4Se3 and toluene by metal(II) macrocyclic complexes, Journal of the Chemical Society Dalton Transactions, pp 2927-2932 (1999)

Asfari, Z., Nicolle, X., Vicens, J., Dozol, J.-F., Duhart, A., Harrowfield, J.M., Skelton, B.W. and White, A.H. Ditopic calixcrowns with inequivalent crown loops: synthesis and structural characterisation of an unsymmetrical calix[4]arenebiscrown-6, Journal of Inclusion Phenomena and Macrocyclic Chemistry, 33: pp 251-262 (1999)

Baker, M.V., Brown, D.H., Skelton, B.W. and White, A.H. Chromium complexes of hydroxyl-functionalised 1,3,5-triazacyclohexanes, Journal of the Chemical Society Dalton Transactions, pp 1483-1490 (1999)

Baker, M.V., Palermo, M.C., Skelton, B.W. and White, A.H. Titanium(IV) imido complexes of 1,3,5-trialkyl-1,3,5-triazacyclohexanes, Australian Journal of Chemistry, 52: pp 179-183 (1999)

Baker, M.V., North, M.R., Skelton, B.W. and White, A.H. Oxidation of (R3tach)M(CO)3 complexes [M = Cr, Mo, W; R3tach = 1,3,5-trialkyl-1,3,5-triazacyclohexane (R = t-Bu, Bn)]. Crystal structures of (t-Bu3tach)MO3.15H2O (M = Mo, W), Inorganic Chemistry, 38: pp 4515-4521 (1999)

Baker, M.V., Bosnich, M.J., Williams, C.C., Skelton, B.W. and White, A.H.Imidazolium-linked cyclophanes, Australian Journal of Chemistry, 52: pp 823-825 (1999)

Bowmaker, G.A., Brown, C.L., Hart, R.D., Healy, P.C., Rickard, C.E.F. and White, A.H. Co-ordination and conformational isomerism in bis(tricyclohexylphosphine)gold(I) halides, Journal of the Chemical Society Dalton Transactions, pp 881-889 (1999)

Bowmaker, G.A., de Silva, E.N., Healy, P.C., Skelton, B.W. and White, A.H.Structural, vibrational and solid state CP MAS 31P NMR spectroscopic studies of complexes of trimethylphosphine with copper(I) and silver(I) halides, Journal of the Chemical Society Dalton Transactions, pp 901-907 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Coupling and disproportionation reactions of ethyne on ruthenium carbonyl clusters: molecular structures of Ru5(µ4-CHCHCCH2)(CO)15 and Ru6(µ-H)(µ4-C)(µ4-CCMe)(µ-CO)(CO)16, Journal of the Chemical Society Dalton Transactions, pp 13-14 (1999)

Bruce, M.I., Kelly, B.D., Skelton, B.W. and White, A.H. Reactions of a ditungsten-capped tetrayne with cobalt carbonyls: molecular structures of {W(CO)3Cp}2{µ-C8[Co2(µ-dppm)m(CO)6-2m]n} (m = 0, 1; n = 1, 2), Journal of the Chemical Society Dalton Transactions, pp 847-852 (1999)

Bruce, M.I., Halet, J.-F., Kahlal, S., Low, P.J., Skelton, B.W. and White, A.H.Reactions of M(CšCCšCR)(CO)3Cp [M = Mo, W; R = H, Fe(CO)2Cp, M(CO)3Cp] with cobalt carbonyls: X-ray structures of {Cp(OC)8Co2M(µ3-C)} CšC{(µ3-C)- Co2M'(CO)8Cp} (M = M' = Mo, W; M = Mo, M' = W), Journal of Organometallic Chemistry, 578: pp 155-168 (1999)

Bruce, M.I., Kühl, O., Skelton, B.W. and White, A.H. Crystal and molecular structures of Ru3(µ-dppm)(CO)9{PPh2(C6H4N=CHPh-2)}, Australian Journal of Chemistry, 52: pp 705-707 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Temperature dependence of the crystal structure of Ru4(µ4-C2H2)(CO)9(h-PhMe), Australian Journal of Chemistry, 52: pp 681-684 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Preparation and structure of Ru2(µ-O2CCF3)2(CO)4(NCMe)2, Australian Journal of Chemistry, 52: pp 621-623 (1999)

Bruce, M.I., Skelton, B.W., Smith, M.E. and White, A.H. Preparation and molecular structures of FcCšCI and {Co2(CO)6}2(µ:µ-FcC2C2Fc) [Fc = ferrocenyl, (h-C5H4)Fe(h-C5H5)], Australian Journal of Chemistry, 52: pp 431-435 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N Reactions of Ru3(CO)12 with ethyne: molecular structure of Ru2(µ-h1,h4:h1,h4-C8H8)(CO)4, Australian Journal of Chemistry, 52: pp 413-415 (1999)

Bruce, M.I., Hall, B.C., Kelly, B.D., Low, P.J., Skelton, B.W. and White, A.H.An efficient synthesis of polyynyl and polyyndiyl complexes of ruthenium(II), Journal of the Chemical Society Dalton Transactions, pp 3719-3728 (1999)

Bruce, M.I., Zaitseva, N.N., Skelton, B.W. and White, A.H. Auration of [Ru3(µ-H)(µ3-C2H)(CO)9]: tetrahedral and butterfly isomers of [AuRu3(µ-H)(µ3-HC2H)(CO)9(PPh3)] and related chemistry, Journal of the Chemical Society Dalton Transactions, pp 2777-2783 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Reactions of Ru3(CO)10(NCMe)2 with ethyne: molecular structures of some prototypical cluster complexes, Journal of the Chemical Society Dalton Transactions, pp 1445-1453 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. An unusual intramolecular metallalactone formation from coordinated alkoxide and CO: molecular structure of Au3Ru3{µ-h1:h1:h1, h2-CCHCPh2OC(O)}(CO)8(PPh3)3, Inorganic Chemistry Communications, 2: pp 453-455 (1999)

Bruce, M.I., Skelton, B.W., White, A.H. and Zaitseva, N.N. Migration of phenyl from dppm to allenylidene and cyclisation to 1,3-diarylindenyl on an Ru3 cluster, Inorganic Chemistry Communications, 2: pp 17-20 (1999)

Bruce, M.I., Hall, B.C., Low, P.J., Skelton, B.W. and White, A.H. Some ruthenium complexes derived from 1,4-diethynylbenzene: molecular structure of Ru{h3-C[=C(CN)2] C(C6H4CšCH-4)=C(CN)2}(PPh3)Cp, Journal of Organometallic Chemistry, 592: pp 74-83 (1999)

Bruce, M.I., Mingzhe, K., Kelly, B.D., Low, P.J., Smith, M.E., Skelton, B.W. and White, A.H. Syntheses of complexes containing substituted 4-ethynylquinolines or 1-azabuta-1,3-dienes by addition of imines to a cationic butatrienylidene-ruthenium complex, Journal of Organometallic Chemistry, 590: pp 184-201 (1999)

Bruce, M.I., Humphrey, P.A., Skelton, B.W. and White, A.H. Migration of a phenyl group from coordinated CH2(PPh2)2 to an acetylide on an Ru3 cluster: X-ray structure of [Ru3(µ-H)(µ3-PPhCH2PPh2)(µ3-PhC2But)(CO)6], Journal of the Chemical Society Dalton Transactions, pp 479-486, 1701 (1999)

Byrne, L.T., Hos, J.P., Koutsantonis, G.A., Skelton, B.W. and White, A.H. Reactions of metalloalkynes 5. Reinvestigation of the reaction of [{Ru(CO)2(h-C5H4R)}2(µ-CšC)] with [Ru3(CO)10(µ-dppm)]., Journal of Organometallic Chemistry, 592: pp 95-102 (1999)

Canty, A.J., Jin, H., Skelton, B.W. and White, A.H. Platinum-tin bonded complexes, including a structural analysis of the octahedral tris(pyrazol-1-yl)borate complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"}, Australian Journal of Chemistry, 52: pp 417-419 (1999)

Canty, A.J., Dedieu, A., Hong, J., Milet, A., Skelton, B.W., Trofimenko, S. and White, A.H. Coordination geometries for palladium and platinum: theoretical studies and the synthesis and structure of tris(indazol-1-yl)borate complexes MMe3{(ind)3BH}, Inorganica Chimica Acta, 287: pp 27-36 (1999)

Canty, A.J., Hoare, J.L., Patel, J., Pfeffer, M., Skelton, B.W. and White, A.H.Organoplatinum(IV) and palladium(IV) complexes containing intramolecular coordination systems based on the 8-methylquinolinyl group (mq), including structures of the cation [Pt(mq)Me2(bpy)]+ (bpy = 2,2'-bipyridine) and the palladium(IV) complexes Pd(mq)MeR{(pz)2BH2} (R = Me, Ph; [(pz)2BH2]– = bis(pyrazol-1-yl)borate), Organometallics, 18: pp 2660-2667 (1999)

Cingolani, A., Effendy, Marchetti, F., Pettinari, C., Skelton, B.W. and White, A.H.Synthesis and structural systematics of mixed triphenylphosphine/imidazole base adducts of silver(I) oxyanion salts, Journal of the Chemical Society Dalton Transactions, pp 4047-4056 (1999)

Cohen, R.J., McNeal, J.E., Redmond, S.L., Meehan, K., Thomas, R., Wilce, M. and Dawkins, H.J. Luminal contents of benign and malignant prostatic glands: correspondence to altered secretory mechanisms, Human Pathology, 31: pp 94-100 (1999)

Cosgriff, J.E., Deacon, G.B., Delbridge, E.E., Jones, C., Skelton, B.W. and White, A.H. Recent advances in the syntheses and structures of some lanthanoid group 15 heterocyclic complexes, Materials Science Forum, 315-317: pp 136-143 (1999)

Deacon, G.B., Kepert, C.M., Sahely, N., Skelton, B.W., Spiccia, L., Thomas, N.C. and White, A.H. Synthesis and structures of photodecarbonylated ruthenium(II) complexes - potential intermediates for mixed ligand complexes., Journal of the Chemical Society Dalton Transactions, pp 275-277 (1999)

Deacon, G.B., Gitlits, A., Skelton, B.W. and White, A.H. The first neutral homoleptic lanthanoid pyrazolates, including the mixed oxidation state species [Yb2(But2pz)5] (But2pz = 3,5-di-tert-butylpyrazolate), from a simple new synthesis of pyrazolate complexes, Chem. Commun. (Cambridge), :13, pp 1213-1214 (1999)

Deacon, G.B., Delbridge, E.E., Forsyth, C.M., Junk, P.C., Skelton, B.W. and White, A.H. Main group pyrazolates- the X-ray structures of [Al(h2- pz)3], [SnMe3(h 1-Ph2pz)], and [GePh3(h 1- pz)] (R2pz = 3,5-disubstituted pyrazolate), Australian Journal of Chemistry, 52: pp 733-739 (1999)

Deacon, G.B., Forsyth, C.M., Junk, P.C., Skelton, B.W. and White, A.H. The striking influence of intramolecular lanthanoid-p-arene interactions on the structural architecture of the homoleptic aryloxolanthanoid(II) complexes [Eu2(Odpp)(µ-Odpp)3] and [Yb2(Odpp)2(µ-Odpp)2] and the Yb(II)/Yb(III) trimetallic [Yb2(µ-Odpp)3]+[Yb(Odpp)4]– (–Odpp = 2,6-diphenylphenolate), Chemistry – A European Journal, 5: pp 1452-1459 (1999)

Deacon, G.B., Delbridge, E.E., Skelton, B.W. and White, A.H. Organoamido and aryloxo-lanthanoids, 19. Synthesis and structures of cisoid and transoid bis(1,2-dimethoxyethane)bis(h2-pyrazolato)lanthanoid(II) complexes, European Journal of Inorganic Chemistry, pp 751-761 (1999)

Devery, M.P., Dickson, R.S., Skelton, B.W. and White, A.H. Coordination and rearrangement of some organic chalcogenides on a rhodium-rhodium bond; reactions with some strained ring cyclic thioethers and with selenium and tellurium ligands, Organometallics, 18: pp 5292-5298 (1999)

Geue, R.J., Qin, C.J., Ralph, S.F., Sargeson, A.M., Skelton, B.W., White, A.H. and Willis, A.C. Sterically induced transmutations in cobalt amine chemistry, Chemical Communications, pp 2351-2352 (1999)

Jeoffreys, G., Ung, A.T., Pyne, S.G., Skelton, B.W. and White, A.H. Synthesis of thiazole analogues of the immunosuppressive agent (1R,2S,3R)-2-acetyl-4(5)-(1,2,3,4-tetrahydroxybutyl)imidazole, Journal of the Chemical Society Perkin Transactions I, :16, pp 2281-2291 (1999)

Junk, P.C., Kepert, C.J., Wei-Min, LU, Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. X. ('Maximally') hydrated rare earth acetates, Australian Journal of Chemistry, 52: pp 437-457 (1999)

Junk, P.C., Kepert, C.J., Wei-Min, LU, Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XI . ('Maximally') hydrated rare earth(III) trifluoro- and trichloro-acetates, Australian Journal of Chemistry, 52: pp 459-479 (1999)

Junk, P.C., Kepert, D.L., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XIII. ('Maximally') hydrated (heavy) rare earth nitrates, Australian Journal of Chemistry, 52: pp 497-505 (1999)

Junk, P.C., Kepert, C.J., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XX. (Maximally) hydrated rare earth sulfates and the double sulfates, Australian Journal of Chemistry, 52: pp 601-615 (1999)

Junk, P.C., Semenova, L.I., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XVI. (Maximally) hydrated rare earth(III) bromides, Australian Journal of Chemistry, 52: pp 531-538 (1999)

Kepert, C.J., Wei-Min, LU, Semenova, L.I., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XII. Solvated 1:1 adducts of some lanthanoid(III) carboxylates with 1,10-phenanthroline and 2,2':6',2"-terpyridine, Australian Journal of Chemistry, 52: pp 481-496 (1999)

Kepert, C.J., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XXI Polymeric sodium bis(thiodiglycollato)neodymiate(III), Australian Journal of Chemistry, 52: pp 617-620 (1999)

McGuinness, D.S., Cavell, K.J., Skelton, B.W. and White, A.H. Zerovalent palladium and nickel complexes of heterocyclic carbenes: oxidative addition of organic halides, carbon-carbon coupling processes, and the Heck reaction, Organometallics, 18: pp 1596-1605 (1999)

Mislin, G., Graf, E., Hosseini, M.W., Bilyk, A., Hall, A.K., Harrowfield, J.M., Skelton, B.W. and White, A.H. Thiacalixarenes as cluster keepers: synthesis and structural analysis of a magnetically coupled tetracopper(II) square, Chemical Communications, pp 373-374 (1999)

Nowak, K.J., Anderson, J.R., Verity, C.M., North, K.N., Iannaccone, S.T., Muller, C.R., Nurnberg, P., Muntoni, F., Sewry, C., Hughes, I., Sutphen, R., Wattanasirichaigoon, D., Lacson, A.G., Swoboda, K.J., Vigneron, J., Wallgren-Pettersson, C., Beggs, A.H., Laing, N.G., Goebel, H.H., Wilce, M., Pelin, K., Donner, K., Jacob, R.L., Hübner, C. and Oexle, K. Mutations in the skeletal muscle a-actin gene in patients with actin myopathy and nemaline myopathy, Nature Genetics, 23: pp 208-212 (1999)

Semenova, L.I. and White, A.H. Structural systematics of rare earth complexes. XIV. Hydrated 1:1 adducts of lanthanoid(III) nitrates with 2,2':6',2"-terpyridyine, Australian Journal of Chemistry, 52: pp 507-517 (1999)

Semenova, L.I. and White, A.H. Structural systematics of rare earth complexes. XVII. Hydrated 1:1 adducts of 2,2':6',2" - terpyridine with the lanthanoid(III) bromides and some binuclear hydroxy-bridged dimers, Australian Journal of Chemistry, 52: pp 539-550 (1999)

Semenova, L.I. and White, A.H. Structural systematics of rare earth complexes. XIX. (Hydrated) 1:2 mononuclear adducts of lanthanoid(III) chlorides with, Australian Journal of Chemistry, 52: pp 571-600 (1999)

Semenova, L.I., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XVIII. (Hydrated) mononuclear 1:1 adducts of lanthanoid(III) chlorides with, Australian Journal of Chemistry, 52: pp 551-569 (1999)

Semenova, L.I., Sobolev, A.N., Skelton, B.W. and White, A.H. Structural systematics of rare earth complexes. XV. Tris(2,2':6',2"-terpyridine)lanthanoid(III) tris(perchlorate) complexes, Australian Journal of Chemistry, 52: pp 519-529 (1999)

Streltsov, V.A. and Ishizawa, N. Synchrotron X-ray study of the electron density in RFeO3 (R = Nd, Dy), Acta Crystallographica Section B, B55: pp 1-7 (1999)

Streltsov, V.A., Konovalova, E.S. and Paderno, Y.B. Synchrotron electron density probe of strongly correlated electron systems, Physica B, 259-261: pp 1155-1156 (1999)

Streltsov, V.A. and Ishizawa, N. Synchrotron X-ray analysis of the electron density in HoFe2, Acta Crystallographica Section B, B55: pp 321-326 (1999)

Conference Publications

Streltsov, V.A. Synchrotron X-ray study of electron density in magnetic materials, Second Magneto-Electronics International Symposium, Nagano, Japan, Shinkyo Insatsu Inc, pp 303-306 (1999)

Others

Oakley, A.J., Martinac, B. and Wilce, M.C. (Review)Structure and function of the bacterial mechanosensitive channel of large conductance, Protein Science, 8: pp 1915-1921, New York, USA (1999)